Trimethylsilyl trifluoromethanesulfonate

CAS: 27607-77-8

Category: Organosilicon Compounds

PurityReagent Grade ≥99%, Ultra-Dry Grade ≥99.5%
Molecular FormulaC4H9F3O3SSi
Molecular Weight222.26
AppearanceColorless to pale yellow liquid, but often darkens to brown over time
Packaging25 g/glass bottle, 100 g/glass bottle, or 200 kg/steel drum with polyethylene liner
Testing IndicatorsAppearance — Visual inspection; Purity — GC; Moisture — Karl Fischer titration; Identification — FTIR (SO₃ ~1360 cm⁻¹, Si–O–S band); Reactivity — Silylation test with alcohol standard.
Storage NotesStore in a cool, dark, dry, and well-ventilated place (often recommended <15℃). It is highly corrosive (causes severe burns) and reacts violently with water (moisture-sensitive). Keep the container tightly closed under an inert gas atmosphere, away from heat, sparks, and flame.
Lead Time
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days
One of the most powerful and versatile silylating agents, acting as a Lewis Acid catalyst and a strong TMS source. It is widely used in organic synthesis for highly efficient silylation reactions, protection of OH groups, and as a catalyst for reactions like the formation of silyl enol ethers and glycosylation.